Skip to content
Analytical Services

Every assay, and the question it answers

Choose analyses per sample. Most release programmes pair purity with identity and net content; contamination panels are added where the application demands them.

01

Purity

RP-HPLC / UV-DAD

Reverse-phase gradient separation with diode-array detection. Reports main-peak area percent and resolves related substances down to 0.05% area.

Price

$200.00

per sample

Turnaround

3-5 business days

02

Identity Confirmation

LC-MS (ESI-QTOF)

Monoisotopic mass confirmation against the theoretical sequence mass, with charge-state deconvolution and mass-accuracy reporting in ppm.

Price

$150.00

per sample

Turnaround

3-5 business days

03

Net Peptide Content

Quantitative HPLC vs. reference standard

Absolute mass of active peptide per vial, quantified against a certified reference standard. Distinguishes label claim from net peptide delivered.

Price

$125.00

per sample

Turnaround

4-6 business days

04

Sterility

Dedicated vial

USP <71> membrane filtration

14-day incubation across two growth media for aerobic, anaerobic and fungal recovery. Consumes a dedicated unopened vial.

Price

$150.00

per sample

Turnaround

16-18 business days

05

Bacterial Endotoxins

Dedicated vial

USP <85> kinetic chromogenic LAL

Quantitative endotoxin burden in EU/mg with positive product control to demonstrate absence of assay inhibition or enhancement.

Price

$175.00

per sample

Turnaround

5-7 business days

06

Elemental Impurities

ICP-MS, USP <232>/<233>

Class 1 and Class 2A elemental impurities - lead, arsenic, cadmium, mercury, plus catalytic residues - quantified to sub-ppb detection limits.

Price

$100.00

per sample

Turnaround

5-7 business days

07

Residual Solvents

GC-HS-FID, USP <467>

Static headspace screen for Class 1 and Class 2 synthesis solvents including acetonitrile, DMF, TFA-associated residues and methanol.

Price

$135.00

per sample

Turnaround

5-7 business days

08

Vial Conformity

Billed per vial

Dimensional & closure inspection

Fill volume, closure integrity, crimp seal and cake appearance assessed per vial against your specification.

Price

$50.00

per vial

Turnaround

2-3 business days

09

Documented Vial Photography

Included free

Calibrated macro imaging

High-resolution as-received imaging of the vial, label and lyophilised cake, appended to the Certificate of Analysis at no charge.

Price

Free

per sample

Turnaround

Included

Instrumentation

The platforms behind each result

RP-HPLC

Purity & related substances

Gradient reverse-phase separation with diode-array detection. Resolves related substances to 0.05% area and reports main-peak purity against a validated method.

0.05%
LOQ, area

LC-MS

Identity confirmation

Electrospray QTOF mass spectrometry confirms monoisotopic mass against the theoretical sequence, with charge-state deconvolution and ppm accuracy reporting.

< 5 ppm
Mass accuracy

ICP-MS

Elemental impurities

USP <232>/<233> elemental impurity panel covering Class 1 and Class 2A elements plus catalytic residues, quantified to sub-ppb detection limits.

ppb
Detection limit

Sterility Testing

USP <71>

Membrane filtration with a 14-day incubation across two growth media, covering aerobic, anaerobic and fungal recovery under validated aseptic technique.

14 days
Incubation

Endotoxin

USP <85> kinetic chromogenic

Quantitative bacterial endotoxin determination in EU/mg, with positive product control demonstrating absence of assay inhibition or enhancement.

0.005 EU/mL
Sensitivity

Heavy Metals

Lead, arsenic, cadmium, mercury

Targeted quantification of the four heavy metals of greatest toxicological concern, with microwave digestion and matrix-matched calibration.

4 elements
Core panel

Residual Solvents

USP <467>, GC-HS-FID

Static headspace gas chromatography screening for Class 1 and Class 2 synthesis solvents, including acetonitrile, DMF, methanol and TFA-associated residues.

Class 1 & 2
Coverage

Net Content

Quantitative peptide assay

Absolute active peptide mass per vial against a certified reference standard - the difference between what the label claims and what the vial delivers.

± 2%
Repeatability

Detection limits and working ranges are method- and matrix-specific. The figures above describe typical performance under our validated conditions; your reported limits appear on your certificate.

Planning your shipment

How many vials to send

Chromatographic and spectrometric assays can share material from a single vial. Sterility and bacterial endotoxin testing cannot - each consumes a dedicated, unopened vial, because the question they answer is destroyed by the first entry.

The submission form performs this arithmetic as you select assays and states your total vial count before you confirm. Sending too few vials is the most common cause of delay on an otherwise complete order.

Read the full explanation

Worked example

  • Purity + Identity + Net Content1 vial
  • + Bacterial Endotoxins+1 vial
  • + Sterility+1 vial
  • Total to ship3 vials

Vial conformity inspection is billed per vial and applies to every vial you send, including the dedicated ones.